Dc.contributor.author Kuswandi, M. Dc.contributor.author Kusumaningtyas, Erwinda dc.contributor.author Santoso, Broto dc.date.accessioned 2016-10-21T09:07:34Z dc.date.available 2016-10-21T09:07:34Z dc.date.issued 2016-08-27 dc.identifier.citation Amalia, D., Ngadiwiyana, danFachriyah, F., 2013, SintesisEtilSinamatdariSinamaldehidpad aMinyakKayu Manis (Cinnamomum cassia) danUjiAktivitassebagaiAntidiabetes, JurnalSainsdanMatematika.
Creative Commons License This work is licensed under a Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License. Jurnal Internasional Sci. 86, Halaman 25: Sintesis dan Sitotoksisitas Evaluasi Novel Asimetris Mono-Carbonyl Analog dari Curcumin (AMACs) terhadap Vero, HeLa, dan MCF7 Cell Lines Jurnal Internasional Penyakit hati kronis anak: Sebuah studi klinikopatologis dari pusat perawatan tersier.
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FMIPA Universitas Indonesia. Fitrianti E., 2008 Sintesis Ester Fruktovanilat dari Fruktosa dan Asam Vanilat Menggunakan Gelombang Mikro Serta Uji Aktivitas Antioksidan, Skripsi, FMIPA, Universitas Indonesia. Et al., 2014. Synthesis and Biolagical Evaluation of Gallic acid Peptide Derivates. Res., 04, pp.16–21.
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Boca Raton, FL. Et al, 2005, Synthesis of a Novel Plant Growth Promoter from Gallic Acid, India, Bioorganic and Medicinal Chemistry Letters, 15: 1243-1247.
Pavia,D.L., Lapman, G.M., Kriz, G.S., Dan Vyvyan,J.A., 2008, Introduction to Spectroscopy, 4thedition, Brooks Cole. Prasetyaningrum, Utami, R., dan Anandito, R.B.K.,2012. Aktivitas Antioksidan, Total Fenol, dan Antibakteri Minyak Atsiri dan Oleoresin Kayu Manis (Cinnamomum burmanii), Jurnal teknosains pangan, ISSN.2302-0733. Sarker, D.Satyajit., dan Nahar, Lutfun., 2009, Kimia untuk mahasiswa farmasi: Bahan kimia organik, Alam dan Umum, Terjemahan dari Chemistry For Pharmacy Students: General Organic and Natural Product Chemistry, oleh Wiley, John., and Ltd, Son., Pustaka Pelajar, Yogyakarta Sawant, N.R.
Dan Chavan, A.R., 2013. Determination of Gallic Aid from Their Methabolic Extract of Punica granatum by HPLC method. International Journal of ChemTech Research, CODEN USA, ISSN. Siddharth S., 2005, Design, synthesis and antimicrobial evaluation of amino acid and peptide derivates of 7- aminocephalosporanic acid, Thesis, Rajiv Gandhi University of Health Sciences, Karnataka, Banga lore. InID dc.identifier.issn 2407-9189 dc.identifier.uri dc.description.abstract A drug compounds can be obtained through synthesis by modifying the structure of potential. Gallic acid and cinnamaldehyde alleged to have potent antioxidant activity.
If two compounds are combined is expected to form a compound that increase the activity by synergy rule. The synthesis involves reacting 5 mmol of gallic acid with 22 mmolcinnamaldehyde using concentrated sulfuric acid as catalyst. The mixtureof reactant was inserted to the microwave for 2 minutes. The product was stored in a temperature 8 ⁰ C for 24 hours to obtain a precipitate. The precipitate was dried and tested its melting point value, TLC and IR.The result of the melting point of the target molecule ranges from 124.7-183,2ºC showed that the product obtained is not pure.
Results of thin layer chromatography and IR indicating the presence of a new compound that forms marked by the value of Rf 0.68 in the mobile phase of methanol:water (3: 1) in the reverse phase system and Rf 0.76 in the mobile phase n-hexane: ethyl acetate: methanol (4: 6: 20μL) in the normal phase system. The target compound had a specific marker peak ester group (C-O) at a frequency of 1249.87 and 1195.87 that were not represented by starting material. The results formed the yield of 76.35%. The results demonstrated that the (2E) -3- phenylprop-2-enoyl-3,4,5-trihydroxybenzoatecould be synthesized using microwave method inID dc.language.iso id inID dc.publisher STIKES Muhammadiyah Pekajangan inID dc.subject Heating inID dc.subject Gallic acid, Cinnamaldehyde inID dc.subject Microwave inID dc.subject (2E) -3- fenilprop-2-enoil 3,4,5- trihidroksibenzoat inID dc.title Sintesis Senyawa (2E)-3-Fenilprop-2-Enoil 3,4,5- Trihidroksibenzoat Dengan Menggunakan Microwave inID dc.type Article inID Files in this item.
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